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当前位置: 安谱实验 > 解决方案 > 安谱实验科技:婴幼儿配方食品中的维生素D2的检测

安谱实验科技:婴幼儿配方食品中的维生素D2的检测

2017/11/25 15:04

阅读:63

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应用领域:
食品/农产品
发布时间:
2017/11/25
检测样品:
婴幼儿谷粉产品
检测项目:
营养成分
浏览次数:
63
下载次数:
参考标准:
UV-HPLC

方案摘要:

婴幼儿配方食品中的维生素D2的检测,方法如下: 样品前处理: 1g 奶粉样品,用5mL 乙腈处理沉淀蛋白,旋转混合2 分钟,6000rpm 离心5 分钟; 取出上清液,重复操作一次,合并两次上清液。上清液吹干,用1mL 水定容,固相萃取待净化。 SPE 活化: 5mL 甲醇 (SBEQ-CA1154 CNWBOND CYH 环己烷 SPE 小柱500mg,6mL/30 pcs) 平衡: 5mL 水 上样: 流速1d/S 淋洗: 5 mL 5% 甲醇水溶液 洗脱: 5mL 甲醇(收集)流速1d/S 定容: 洗脱液在40 ℃ 下氮吹干,用1mL 甲醇定容,SCAA-113 过滤, 待液相色谱检测

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婴幼儿配方食品中的维生素23的检测.pdf
917KB
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